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SUMMARY:Contr. Talk 13 - Studying slow dynamics with X-ray photon correlat
 ion spectroscopy
DTSTART;VALUE=DATE-TIME:20181212T103000Z
DTEND;VALUE=DATE-TIME:20181212T105000Z
DTSTAMP;VALUE=DATE-TIME:20260523T191708Z
UID:indico-contribution-94-483@lindico453.srv.lu.se
DESCRIPTION:Speakers: Oier Bikondoa (ESRF-The European Synchrotron\, Greno
 ble\, France)\nScattering experiments based on coherent X-ray beams have o
 pened new possibilities for the investigation of soft and hard condensed m
 atter. X-ray photon correlation spectroscopy (XPCS) allows to access a wid
 e variety of dynamic phenomena at the nanoscale by studying the temporal c
 orrelations among photons that are scattered by a material when it is illu
 minated using a coherent X-ray beam. \nWe present two examples of XPCS stu
 dies on systems with slow dynamics that illustrate the capabilities of the
  technique in SAXS and GISAXS geometries: (a) Dynamics of ion beam eroded 
 surfaces\, which represent a paradigmatic case of sustained non-equilibriu
 m dynamics governed by the complex interplay between the mechanisms that t
 end to roughen and smoothen the surface [1]\; (b) An ongoing study on the 
 initial steps of self-assembly mechanism and gelation of a pH-sensitive lo
 w molecular weight  hydrogelator\, controlling both assembly rate and morp
 hology of the self-assembled structures.\nWe shall also discuss on the ben
 efits and possibilities that the new diffraction limited storage rings bri
 ng about for XPCS studies.\n\nhttps://lindico453.srv.lu.se/event/67/contri
 butions/483/
LOCATION:Elite Hotel Ideon Tera
URL:https://lindico453.srv.lu.se/event/67/contributions/483/
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BEGIN:VEVENT
SUMMARY:Contr. Talk 12 - Effect of confinement on lyotropic lamellae dynam
 ics under shear flow
DTSTART;VALUE=DATE-TIME:20181212T101000Z
DTEND;VALUE=DATE-TIME:20181212T103000Z
DTSTAMP;VALUE=DATE-TIME:20260523T191708Z
UID:indico-contribution-94-482@lindico453.srv.lu.se
DESCRIPTION:Speakers: Luigi Gentile (Department of Biology\, Microbial Eco
 logy Group\, Lund University)\nLyotropic lamellar phases under shear flow 
 show surprising changes in the microscopic structures and physical propert
 ies. Lamellae-to-multi-lamellar-vesicle (MLV) transition has been widely i
 nvestigated\, whereas lamellae tilting and vesicles inclination have not b
 een highlighted during this kind of transition. Flow instabilities and the
 ir correlation with structures and properties in a confined gap is also ma
 tter of investigation. Here time-resolved flow-small angle neutron scatter
 ing (SANS) experiments have been carried out using a 1-2 shear cell to det
 ect inclination and deformation of the MLVs and to correlate spatially dis
 tributed structures in the Couette gap with progressive evolution of the l
 ocal viscosity towards two significantly different values\, leading to sta
 ble and periodic viscosity oscillations. The inclination angle of the MLVs
  has been addressed in terms of capillary number and its spatial behavior 
 along the Couette gap in terms of gap confinement.\n\nhttps://lindico453.s
 rv.lu.se/event/67/contributions/482/
LOCATION:Elite Hotel Ideon Tera
URL:https://lindico453.srv.lu.se/event/67/contributions/482/
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SUMMARY:Keynote 11 - Development of µRheoSANS and Investigating the Struc
 ture and Rheology of Complex Fluids at High Shear Rate
DTSTART;VALUE=DATE-TIME:20181212T093000Z
DTEND;VALUE=DATE-TIME:20181212T101000Z
DTSTAMP;VALUE=DATE-TIME:20260523T191708Z
UID:indico-contribution-94-481@lindico453.srv.lu.se
DESCRIPTION:Speakers: Katie Weigandt (National Inst. of Science and Techno
 logy  Center for Neutron Research\, USA)\nWe are developing slit rheometer
 s compatible with simultaneous small angle neutron scattering (SANS) measu
 rements to directly correlate structure and rheology over a broad range of
  conditions. Eventually we hope to probe sample structure in Poiseuille fl
 ow at high shear rates\, under high pressure head\, and relatively high te
 mperatures. This builds upon an existing suite of Couette rheoSANS and flo
 wSANS devices at the NIST Center for Neutron Research that are accessible 
 to the scientific community through a peer reviewed proposal system. Indus
 trial applications\, such as lubrication\, mixing\, spraying and injection
 \, involve the flow of complex fluids at high deformation rates. Clogging\
 , fluid degradation\, and other processing challenges can arise in these e
 xtreme contexts and are often driven by structural changes in the fluid. T
 o date\, we have developed a prototype slit rheometer capable of simultane
 ously measuring structure and rheology of relatively low viscosity or shea
 r thinning fluids (η∞ < 5 mPa∙s) at shear rates up to 100\,000 s-1 an
 d a capillary rheoSANS instrument capable of simultaneously measuring stru
 cture and rheology at rates up to 106 s-1. Our initial investigations have
  focused on measuring wormlike micelle solutions at low to moderate shear 
 rates and comparing the results with Couette rheoSANS measurements. In thi
 s talk we will discuss the ongoing development of µRheoSANS measurements 
 including our existing low-pressure apparatus\, the capillary device and o
 ur newly built high pressure µRheoSANS device\, designed to withstand pre
 ssure drops or pressure heads up to 350 bar. This device will enable us to
  measure SANS at shear rates up to 106 in samples with η∞ ~ 100 mPa∙s
 . Furthermore\, we will discuss the results of a series of experiments aim
 ed at understanding the rheological response of wormlike micelle solutions
  at relatively high shear rates.\n\nhttps://lindico453.srv.lu.se/event/67/
 contributions/481/
LOCATION:Elite Hotel Ideon Tera
URL:https://lindico453.srv.lu.se/event/67/contributions/481/
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